東華分析——鐵氰.化.鉀在玻碳電極上的氧化還原行為

打開瀏覽(lan)器東(dong)華自(zi)測PC軟件，導(dao)致表面：

打(da)開網頁(ye)右上角 電腦硬件：發生表(biao)面：

點選IP配置，將(jiang)外面的(de)IP改成(cheng)為(wei)192.168.0.95：

單擊找尋按健，左(zuo)下角表明連(lian)上測量儀器：

進(jin)(jin)行拼(pin)接電解(jie)拋(pao)光池(chi)：將電電學工作(zuo)的(de)站WE和(he)SE短接（撥(bo)掉SE下面的(de)鄂(e)(e)魚夾，插入表格(ge)WE鄂(e)(e)魚夾后(hou)孔內因此WE和(he)SE短接）進(jin)(jin)行拼(pin)接玻碳金(jin)屬電級(ji)(ji)，RE進(jin)(jin)行拼(pin)接參比金(jin)屬電級(ji)(ji)，CE進(jin)(jin)行拼(pin)接對金(jin)屬電級(ji)(ji)。

點擊事(shi)件【自動測(ce)量】控制(zhi)鍵中的(de)新實(shi)驗英(ying)文，實(shi)操選定擇反復(fu)的(de)伏安法（多反復(fu)的(de)），顯示這(zhe)用(yong)戶界面；

更(geng)變(bian)網頁產品參數，剛開(kai)始(shi)的(de)電(dian)(dian)(dian)(dian)(dian)極電(dian)(dian)(dian)(dian)(dian)勢差為(wei)-0.2V，端點(dian)電(dian)(dian)(dian)(dian)(dian)極電(dian)(dian)(dian)(dian)(dian)勢差1為(wei)-0.2V，端點(dian)電(dian)(dian)(dian)(dian)(dian)極電(dian)(dian)(dian)(dian)(dian)勢差2為(wei)0.7V，最終能夠電(dian)(dian)(dian)(dian)(dian)極電(dian)(dian)(dian)(dian)(dian)勢差為(wei)-0.2V，間(jian)歇(xie)(xie)兩(liang)次5次，靜置時光(guang)0s，復印機測試傳輸率0.05V/s，間(jian)歇(xie)(xie)兩(liang)次5次（暗示著著復印機測試4個間(jian)歇(xie)(xie)），感(gan)(gan)應(ying)電(dian)(dian)(dian)(dian)(dian)壓工作電(dian)(dian)(dian)(dian)(dian)流量(liang)量(liang)量(liang)限(xian)(xian)(xian)也都(dou)就可以完(wan)成(cheng)定(ding)時，也也都(dou)就可以完(wan)成(cheng)手動式量(liang)限(xian)(xian)(xian)，也都(dou)就可以合(he)理完(wan)成(cheng)1mA量(liang)限(xian)(xian)(xian)，調(diao)查(cha)(cha)所(suo)性完(wan)成(cheng)一些(xie)間(jian)歇(xie)(xie)后，如(ru)何查(cha)(cha)看(kan)感(gan)(gan)應(ying)電(dian)(dian)(dian)(dian)(dian)壓工作電(dian)(dian)(dian)(dian)(dian)流量(liang)量(liang)最明(ming)(ming)顯值(zhi)，進而開(kai)始(shi)和結束(shu)調(diao)查(cha)(cha)所(suo)性，感(gan)(gan)應(ying)電(dian)(dian)(dian)(dian)(dian)壓工作電(dian)(dian)(dian)(dian)(dian)流量(liang)量(liang)量(liang)限(xian)(xian)(xian)就完(wan)成(cheng)超(chao)過感(gan)(gan)應(ying)電(dian)(dian)(dian)(dian)(dian)壓工作電(dian)(dian)(dian)(dian)(dian)流量(liang)量(liang)最明(ming)(ming)顯值(zhi)的(de)量(liang)限(xian)(xian)(xian)必須(xu)，舉個例(li)子來說一些(xie)間(jian)歇(xie)(xie)調(diao)查(cha)(cha)所(suo)性中感(gan)(gan)應(ying)電(dian)(dian)(dian)(dian)(dian)壓工作電(dian)(dian)(dian)(dian)(dian)流量(liang)量(liang)最明(ming)(ming)顯值(zhi)發展(zhan)趨勢是90uA差不多，量(liang)限(xian)(xian)(xian)完(wan)成(cheng)100uA必須(xu)。

打(da)開(kai)(kai)網頁【現在準(zhun)(zhun)備】開(kai)(kai)關(guan)(guan)(guan)按鈕(niu)(niu)開(kai)(kai)關(guan)(guan)(guan)圖(tu)(tu)(tu)片(pian)，排(pai)列順序(xu)(xu)后，科(ke)(ke)(ke)學實踐(jian)設(she)(she)計(ji)現在準(zhun)(zhun)備開(kai)(kai)機運行，如何科(ke)(ke)(ke)學實踐(jian)設(she)(she)計(ji)環節中需要關(guan)(guan)(guan)閉程序(xu)(xu)，打(da)開(kai)(kai)網頁【關(guan)(guan)(guan)閉程序(xu)(xu)】開(kai)(kai)關(guan)(guan)(guan)按鈕(niu)(niu)開(kai)(kai)關(guan)(guan)(guan)圖(tu)(tu)(tu)片(pian)，后來(lai)進行快速設(she)(she)置參數設(she)(she)置，打(da)開(kai)(kai)網頁【現在準(zhun)(zhun)備】開(kai)(kai)關(guan)(guan)(guan)按鈕(niu)(niu)開(kai)(kai)關(guan)(guan)(guan)圖(tu)(tu)(tu)片(pian)，進行科(ke)(ke)(ke)學實踐(jian)設(she)(she)計(ji)。

現場實(shi)驗(yan)終止(zhi)后,智能調用(yong)到【分析一下】工具欄，出來上面數字圖像：

選擇右上角的倒三角型按紐，可以點擊(ji)空格選擇(ze)每項次不斷循(xun)環(huan)(huan)的(de)圖像，一(yi)般第一(yi)點次巡(xun)環(huan)(huan)的(de)數據我(wo)們不要，所(suo)以我(wo)們只選擇(ze)segment2, segment3, segment4, segment5。

數據導出，鼠標(biao)點(dian)擊【分析】里面的【導出】鍵，

出現下述視圖，選您要保(bao)留(liu)(liu)的版式，選好的保(bao)留(liu)(liu)部位，保(bao)留(liu)(liu)。

峰值尋(xun)找：選擇結尾(wei)有一次間(jian)歇數據。Ctrl+鼠(shu)標左(zuo)鍵選出峰值位置(zhi)，如圖，

單擊右上端基線研究(jiu)分(fen)析控(kong)制(zhi)鍵(jian)的功能鍵(jian)，出現內容(rong)如下(xia)形象(xiang)：

手動調準幾根(gen)氧化硅線(xian)具體位置，使之(zhi)與切線(xian)交往，可不可以(yi)斷定陽極峰(feng)電(dian)勢、峰(feng)瞬時(shi)電(dian)流(liu)量，陰極峰(feng)電(dian)勢、峰(feng)瞬時(shi)電(dian)流(liu)量。如：

假(jia)如(ru)要緊接著(zhu)做(zuo)實(shi)踐(jian)(jian)，點開右下角【測(ce)量方法】快捷(jie)，后(hou)來采用新實(shi)踐(jian)(jian)，采用大家要做(zuo)的實(shi)踐(jian)(jian)能夠。